A Simple Low-Cost Single-Crystal NMR Setup

TY - JOUR

T1 - A Simple Low-Cost Single-Crystal NMR Setup

AU - Vinding, Mads Sloth

AU - Kessler, Tommy Ole

AU - Vosegaard, Thomas

PY - 2016/8/1

Y1 - 2016/8/1

N2 - A low-cost single-crystal NMR kit is presented along with a web-based post-processing software. The kit consists of a piezo-crystal motor and a goniometer for the crystal, both embedded in a standard wide-bore NMR probe with a 3D printed scaffold. The NMR pulse program controls the angle setting automatically, and the post-processing software incorporates a range of orientation-angle discrepancies present in the kit and other single-crystal setups. Results with a NaNO 3 single-crystal show a high degree of reproducibility and excellent agreement with previous findings for the anisotropic quadrupolar interaction.

AB - A low-cost single-crystal NMR kit is presented along with a web-based post-processing software. The kit consists of a piezo-crystal motor and a goniometer for the crystal, both embedded in a standard wide-bore NMR probe with a 3D printed scaffold. The NMR pulse program controls the angle setting automatically, and the post-processing software incorporates a range of orientation-angle discrepancies present in the kit and other single-crystal setups. Results with a NaNO 3 single-crystal show a high degree of reproducibility and excellent agreement with previous findings for the anisotropic quadrupolar interaction.

KW - 3D print

KW - Goniometer

KW - JavaScript

KW - Piezo motor

KW - Single-crystal NMR

KW - jsNMR

UR - http://www.scopus.com/inward/record.url?scp=84974577147&partnerID=8YFLogxK

U2 - 10.1016/j.jmr.2016.06.004

DO - 10.1016/j.jmr.2016.06.004

M3 - Journal article

C2 - 27295612

SN - 1090-7807

VL - 269

SP - 120

EP - 127

JO - Journal of Magnetic Resonance

JF - Journal of Magnetic Resonance

ER -